In situ forming hydrogels based on thermosensitive polymers have attractive properties for tissue engineering. However, the physical interactions in these hydrogels are not strong enough to yield gels with sufficient stability for many of the proposed applications. In this study, additional covalent cross-links were introduced by photopolymerization to improve the mechanical properties and the stability of thermosensitive hydrogels. Methacrylate groups were coupled to the side chains of triblock copolymers (ABA) with thermosensitive poly( N-(2-hydroxypropyl) methacrylamide lactate) A blocks and a hydrophilic poly(ethylene glycol) B block. These polymers exhibit lower critical solution temperature (LCST) behavior in aqueous solution and the cloud point decreased with increasing amounts of methacrylate groups. These methacrylate groups were photopolymerized above the LCST to render covalent cross-links within the hydrophobic domains. The mechanical properties of photopolymerized hydrogels were substantially improved and their stability was prolonged significantly compared to nonphotopolymerized hydrogels. Whereas non-UV-cured gels disintegrated within 2 days at physiological pH and temperature, the photopolymerized gels degraded in 10 to 25 days depending on the degree of cross-linking. To assess biocompatibility, goat mesenchymal stem cells were seeded on the hydrogel surface or encapsulated within the gel and they remained viable as demonstrated by a LIVE/DEAD cell viability/cytotoxicity assay. Expression of alkaline phosphatase and production of collagen I demonstrated the functionality of the mesenchymal stem cells and their ability to differentiate upon encapsulation. Due to the improved mechanical properties, stability, and adequate cytocompatibility, the photopolymerized thermosensitive hydrogels can be regarded as highly potential materials for applications in tissue engineering.

译文

基于热敏聚合物的原位形成水凝胶对组织工程具有吸引力。然而,这些水凝胶中的物理相互作用不够强,不足以产生对于许多建议的应用具有足够稳定性的凝胶。在这项研究中,通过光聚合引入了其他共价交联,以改善热敏水凝胶的机械性能和稳定性。甲基丙烯酸酯基团与具有热敏性聚 (N-(2-羟丙基) 甲基丙烯酰胺乳酸酯) A嵌段和亲水性聚 (乙二醇) B嵌段的三嵌段共聚物 (ABA) 的侧链偶联。这些聚合物在水溶液中表现出较低的临界溶液温度 (LCST) 行为,并且随着甲基丙烯酸酯基团数量的增加,浊点降低。这些甲基丙烯酸酯基团在LCST上方进行光聚合,以在疏水结构域中形成共价交联。与非光聚合水凝胶相比,光聚合水凝胶的机械性能得到了显着改善,并且其稳定性得到了显着延长。尽管非UV固化的凝胶在生理pH和温度下在2天内崩解,但光聚合的凝胶在10至25天内降解,具体取决于交联程度。为了评估生物相容性,将山羊间充质干细胞接种在水凝胶表面或封装在凝胶内,如活/死细胞活力/细胞毒性测定所证明,它们保持活力。碱性磷酸酶的表达和胶原蛋白I的产生证明了间充质干细胞的功能及其在包封后分化的能力。由于改进的机械性能,稳定性和足够的细胞相容性,光聚合的热敏水凝胶可被视为在组织工程中应用的极具潜力的材料。

+1
+2
100研值 100研值 ¥99课程
检索文献一次
下载文献一次

去下载>

成功解锁2个技能,为你点赞

《SCI写作十大必备语法》
解决你的SCI语法难题!

技能熟练度+1

视频课《玩转文献检索》
让你成为检索达人!

恭喜完成新手挑战

手机微信扫一扫,添加好友领取

免费领《Endnote文献管理工具+教程》

微信扫码, 免费领取

手机登录

获取验证码
登录