Estrogen mediates its effects through multiple cellular receptors. In addition to the classical nuclear estrogen receptors (ERalpha and ERbeta), estrogen also signals through the seven-transmembrane G-protein-coupled receptor (GPCR) GPR30. Although estrogen is a cell-permeable ligand, it is often assumed that all GPCRs function solely as cell surface receptors. Our previous results showed that GPR30 appeared to be expressed predominantly in the endoplasmic reticulum. A critical question that arises is whether this localization represents the site of functional receptor. To address this question, we synthesized a collection of cell-permeable and cell-impermeable estrogen derivatives. We hypothesized that if functional GPR30 were expressed at the cell surface, both permeable and impermeable derivatives would show activity. However, if functional GPR30 were predominantly intracellular, like ERalpha, only the permeable ligands should show activity. Cell permeability was assessed using cells expressing ERalpha as a model intracellular estrogen-binding receptor. Our results reveal that despite exhibiting similar binding affinities for GPR30, only the cell-permeable ligands are capable of stimulating rapid calcium mobilization and phosphoinositide 3-kinase (PI3K) activation. We conclude that GPR30 expressed intracellularly is capable of initiating cellular signaling and that there is insufficient GPR30 expressed on the cell surface to initiate signaling in response to impermeable ligands in the cell lines examined. To our knowledge, this is the first definitive demonstration of a functional intracellular transmembrane estrogen receptor.

译文

雌激素通过多种细胞受体介导其作用。除了经典的核雌激素受体 (ERalpha和ERbeta) 外,雌激素还通过七跨膜g蛋白偶联受体 (GPCR) gpr30发出信号。尽管雌激素是细胞可渗透的配体,但通常认为所有gpcr仅作为细胞表面受体起作用。我们先前的结果表明,GPR30似乎主要在内质网中表达。出现的一个关键问题是,这种定位是否代表功能受体的位点。为了解决这个问题,我们合成了细胞可渗透和细胞不可渗透的雌激素衍生物的集合。我们假设,如果在细胞表面表达功能性GPR30,则可渗透和不可渗透的衍生物都将显示活性。但是,如果功能性GPR30主要是细胞内的,例如ERalpha,则只有可渗透的配体才应显示活性。使用表达ERalpha的细胞作为模型细胞内雌激素结合受体评估细胞通透性。我们的结果表明,尽管对GPR30表现出相似的结合亲和力,但只有细胞可渗透的配体能够刺激快速的钙动员和磷酸肌醇3激酶 (PI3K) 激活。我们得出的结论是,细胞内表达的GPR30能够启动细胞信号传导,并且在细胞表面表达的GPR30不足以响应所检查细胞系中不可渗透的配体来启动信号传导。据我们所知,这是功能性细胞内跨膜雌激素受体的第一个明确证明。

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