Flap endonucleases (FENs) catalyse the exonucleolytic hydrolysis of blunt-ended duplex DNA substrates and the endonucleolytic cleavage of 5'-bifurcated nucleic acids at the junction formed between single and double-stranded DNA. The specificity and catalytic parameters of FENs derived from T5 bacteriophage and Archaeoglobus fulgidus were studied with a range of single oligonucleotide DNA substrates. These substrates contained one or more hairpin turns and mimic duplex, 5'-overhanging duplex, pseudo-Y, nicked DNA, and flap structures. The FEN-catalysed reaction properties of nicked DNA and flap structures possessing an extrahelical 3'-nucleotide (nt) were also characterised. The phage enzyme produced multiple reaction products of differing length with all the substrates tested, except when the length of duplex DNA downstream of the reaction site was truncated. Only larger DNAs containing two duplex regions are effective substrates for the archaeal enzyme and undergo reaction at multiple sites when they lack a 3'-extrahelical nucleotide. However, a single product corresponding to reaction 1 nt into the double-stranded region occurred with A. fulgidus FEN when substrates possessed a 3'-extrahelical nt. Steady-state and pre-steady-state catalytic parameters reveal that the phage enzyme is rate-limited by product release with all the substrates tested. Single-turnover maximal rates of reaction are similar with most substrates. In contrast, turnover numbers for T5FEN decrease as the size of the DNA substrate is increased. Comparison of the catalytic parameters of the A. fulgidus FEN employing flap and double-flap substrates indicates that binding interactions with the 3'-extrahelical nucleotide stabilise the ground state FEN-DNA interaction, leading to stimulation of comparative reactions at DNA concentrations below saturation with the single flap substrate. Maximal multiple turnover rates of the archaeal enzyme with flap and double flap substrates are similar. A model is proposed to account for the varying specificities of the two enzymes with regard to cleavage patterns and substrate preferences.

译文

:Flap内切核酸酶(FENs)催化平末端双链DNA底物的核酸外切水解和单链和双链DNA之间形成的连接处5'-叉状核酸的内切核酸酶裂解。用一系列的单个寡核苷酸DNA底物研究了T5噬菌体和古细菌的FENs的特异性和催化参数。这些底物包含一个或多个发夹转弯和模拟双链体,5'-突出的双链体,假Y,带切口的DNA和襟翼结构。 FEN催化的刻痕DNA和具有螺旋外3'-核苷酸(nt)的襟翼结构的反应特性也得到了表征。噬菌体酶与所有受试底物均产生了不同长度的多种反应产物,除了截短了反应位点下游的双链DNA的长度外。只有包含两个双链体区域的较大的DNA是古细菌的有效底物,并且在缺少3'-螺旋外核苷酸时会在多个位点进行反应。但是,当底物具有3'-extrahelical nt时,对应于反应1 nt进入双链区域的单一产物与A. fulgidus FEN一起出现。稳态和稳态前的催化参数表明,噬菌体酶受所有被测底物的产物释放速率限制。大多数底物的单周转最大反应速率相似。相反,T5FEN的周转数随DNA底物大小的增加而减少。使用襟翼和双襟底物对A. fulgidus FEN的催化参数进行比较表明,与3'-螺旋外核苷酸的结合相互作用稳定了基态FEN-DNA相互作用,从而导致在低于饱和度的DNA浓度下刺激比较反应。单瓣底物。具有皮瓣和双皮瓣底物的古生酶的最大多次转换速率是相似的。提出了一个模型来考虑两种酶在切割模式和底物偏好方面的不同特异性。

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