Extrusion of drugs or drug-like compounds through bacterial efflux pumps is a serious health issue that leads to loss in drug efficacy. Combinatorial therapies of low-efficacy drugs with efflux pump inhibitors may help to restore the activities of such drugs. In this quest, natural products are attractive molecules, since in addition to their wide range of bioactivities they may inhibit efflux pumps. The current work repurposed the bioactive alkaloid roemerine as a potential efflux pump inhibitor. In Bacillus subtilis, both Bmr and BmrA, belonging to the major facilitator and the ATP-binding cassette superfamilies, respectively, were found to be inhibited by roemerine. Scanning electron microscopy and RNA-Seq analyses showed that it potentiated the effect of berberine. Growth rates and checkerboard assays confirmed the synergy of roemerine and berberine and that roemerine prevented berberine efflux by inhibiting Bmr. Transport assays with inverted membrane vesicles prepared from Escherichia coli overexpressing BmrA showed that increasing roemerine concentration decreased the transport of doxorubicin, the BmrA substrate, confirming that roemerine may also be considered as an inhibitor of BmrA. Thus, these findings suggest that conjugation of roemerine to substrates of efflux pumps, Bmr and BmrA, may help to potentiate the activity of their drug substrates.

译文

通过细菌外排泵挤出药物或类药物化合物是一个严重的健康问题,导致药物功效下降。低效药物与外排泵抑制剂的组合疗法可能有助于恢复此类药物的活性。在这一探索中,天然产物是有吸引力的分子,因为除了它们广泛的生物活性外,它们还可能抑制外排泵。当前的工作将生物活性生物碱roemerine重新用作潜在的外排泵抑制剂。在枯草芽孢杆菌中,发现分别属于主要促进剂和ATP结合盒超家族的Bmr和BmrA均被roemerine抑制。扫描电子显微镜和RNA-Seq分析表明,它增强了小檗碱的作用。生长速率和棋盘分析证实了罗梅林和小檗碱的协同作用,并且罗梅林通过抑制Bmr来防止小檗碱的外排。用过表达BmrA的大肠杆菌制备的倒置膜囊泡进行的运输分析表明,增加的roemerine浓度会降低BmrA底物阿霉素的运输,这证实了roemerine也可以被认为是BmrA的抑制剂。因此,这些发现表明,将roemerine与外排泵Bmr和BmrA的底物结合可能有助于增强其药物底物的活性。

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